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Refine Chemicals Science and Technology Developing Co., Ltd.

 
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2-Ethyl-2-Oxazoline

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Product Type:
Intermediates/Synthesis material intermediates
Main Specifications:
no data
Price:
no data
Packing:
The standard packaging is a polyethylene container for 200 kg or as required.
Uses:
no data
Usages:
It is mainly used in Intermediate in organic syntheses. New thermo-responsive polymer materials Poly(2-ethyl-2-oxazoline). Typical procedure. To a flame dried round bottom flask (250mL) fitted with a nitrogen inlet and a rubber septum were added 32 ml of
2-Ethyl-2-Oxazoline Description:  

Chemical name

2-Ethyl-2-oxazoline

INCI name

2-ethyl-4,5-dihydro- Oxazole; 2-Ethyl-2-oxazoline;2-Ethyloxazoline;

CAS-No.

10431-98-8

H.S. Code

29349990

Molecular Formula and weight

C5H9NO 99.13 g/mol

Specification

Appearance clear liquid
Purity 99%min
Flash Point (Deg C ) 29
Moisture 0.2&max
Color <50 APHA

Package

The standard packaging is a polyethylene container for 200 kg or as required.

Storage Conditions

2-Ethyl-2-oxazoline It should be put in cool and dry place. Safety Data R: 11 S: 16-33 F ?Highly Flammable

Applications

2-Ethyl-2-oxazoline It is mainly used in Intermediate in organic syntheses. New thermo-responsive polymer materials Poly(2-ethyl-2-oxazoline). Typical procedure. To a flame dried round bottom flask (250mL) fitted with a nitrogen inlet and a rubber septum were added 32 ml of chlorobenzene and 18 ml (178 mmol) of 2-ethyl-2-oxazoline. At a temperature of 110˚C and under nitrogen the polymerisation was initiated by adding 100 l (0.88 mmol) of methyl triflate The reaction mixture was stirred for 19 hours. During the course of the reaction the solution turned from clear colourless to clear yellow. To the reaction mixture was added 0.8 ml (8.8 mmol) of morpholine. The reaction mixture was stirred for another 4 hours at 110˚C and then cooled down to room temperature. The solution was poured into an excess of cold diethyl ether and the precipitated polymer was isolated by decanting the solvent. The polymer was purified by precipitation from acetonitrile into ether twice.Yield 16.8 g (96%) of a yellow solid. 1H-NMR (CDCl3) showed absence of residual chlorobenzene.

Material Safety Data Sheet

A Material Safety Data Sheet is available.

Note

The data submitted in this publication are based on our current knowledge and experience. They do not constitute a guarantee in the legal sense of the term and, in view of the manifold factors that may affect processing and application, do not relieve those to whom we supply our products from the responsibility of carrying out their own tests and experiments. Any relevant patent rights and existing legislation and regulations must be observed.


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